Camp, Jason, Bousfield, Thomas W., Mistry, Liam and Mapesa, Kopano (2017) Synthesis of ureas in the bio-alternative solvent Cyrene. Green Chemistry. pp. 2123-2128. ISSN 1463-9262
Abstract

Cyrene as a bio-alternative solvent: a highly efficient, waste minimizing protocol for the synthesis of ureas from isocyanates and secondary amines in the bio-available solvent Cyrene is reported. This method eliminated the use of toxic solvents, such as DMF, and established a simple work-up procedure for removal of the Cyrene, which led to a 28-fold increase in molar efficiency versus industrial standard protocols.

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