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The First Preparation of β-Lactones by Radical Cyclization

Castle, Kerstin, Hau, Chee-San, Sweeney, Joseph B. and Tindall, Craig (2003) The First Preparation of β-Lactones by Radical Cyclization. Organic Letters, 5 (5). pp. 757-759. ISSN 1523-7060

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Abstract

β-Lactones have, for the first time, been prepared by 4-exo-trig radical cyclization. Thus, α-ethenoyloxy radicals react in the presence of tributylstannane in a photothermal process to give β-lactones. Highest yields were obtained when groups capable of stabilizing a carbon-centered radical were present at the 3-position of the alkenoate acceptor.

Item Type: Article
Subjects: Q Science > QD Chemistry
Schools: School of Applied Sciences
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Depositing User: Joseph Sweeney
Date Deposited: 18 Oct 2012 11:43
Last Modified: 18 Oct 2012 11:43
URI: http://eprints.hud.ac.uk/id/eprint/15278

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